Hydrochloric Acid → Zirconium(IV) sulfate

HRID 1614859Notes

Reaction equation

HRID 1614859 reaction equation
[S:1]([O-:5])([O-:4])(=[O:3])=[O:2].[Na+].[Na+].O(Cl)Cl.[Zr:11].Cl>>[S:1]([O-:5])([O-:4])(=[O:3])=[O:2].[Zr+4:11].[S:1]([O-:5])([O-:4])(=[O:3])=[O:2]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 24436Sodium SulfateHCID 71304769Chloro hypochlorite;zirconium

Product 1

HCID 26793Zirconium(IV) sulfate

Conditions

Temperature
85 °C

Procedure

141 g of a 25% sodium sulfate solution was heated to 85° C. Then, 375 g of a zirconium oxychloride solution containing 16% of ZrO2 equivalent, previously heated to 85° C., was added thereto. Thereafter, hydrochloric acid was added so that the free acid concentration became 1.5; N, and the resulting product was maintained for 0.5 hour to form basic zirconium sulfate.

Workup

  1. additionwas added
  2. temperatureN, and the resulting product was maintained for 0.5 hour

Sources & evidence

ORD record
ord-2e75669cf5704c02b4b875fbbd2a1ae6
Source dataset
uspto-grants-2014_07
Patent number
US08765631B2

Reaction notes

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