Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromo-2-methoxyphenol | HCID 262234 | — |
| Reactant | (1-Chloropropyl)benzene | HCID 524241 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 59633897 | HCID 59633897 | 99.3% |
Reaction Steps
To a solution of 4-bromo-2-methoxyphenol (7.0 g) and ethylbenzyl chloride (5.6 g) in DMF (35 mL) was added K2CO3 (5.7 g). The reaction mixture was stirred at 80° C. for 1 hr. Water was added to the reaction mixture. The precipitated solid was collected on a filter and dried to give the title compound (11 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08765739B2 |
|---|
| Source dataset | uspto-grants-2014_07 |
|---|
| ORD ID | ord-e0fc5bac5e994aa6a0278294725c99f2 |
|---|
| Source note | uspto-grants-2014_07 |
|---|
