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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1615134Generated: October 28, 2026

HCID 40985380, compound → HCID 67996586, compound

https://huagongshe.com/reaction/1615134

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 40985380HCID 40985380—
Reactant(9-Hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehydeHCID 86668369—
ProductHCID 67996586HCID 6799658660%

Reaction Steps

The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-(4-chloro-phenyl)-propylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 60% of theory; LC (method 5): tR=1.15 min; Mass spectrum (ESI+): m/z=396/398 (Cl) [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765744B2
Source datasetuspto-grants-2014_07
ORD IDord-f91274f618b741a0ba85312e542c967c
Source noteuspto-grants-2014_07