HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 40985380, compound → HCID 67996586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 40985380 | HCID 40985380 | — |
| Reactant | (9-Hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde | HCID 86668369 | — |
| Product | HCID 67996586 | HCID 67996586 | 60% |
Reaction Steps
The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-(4-chloro-phenyl)-propylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 60% of theory; LC (method 5): tR=1.15 min; Mass spectrum (ESI+): m/z=396/398 (Cl) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765744B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-f91274f618b741a0ba85312e542c967c |
| Source note | uspto-grants-2014_07 |