HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 2496556, compound → HCID 67996053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 2496556 | HCID 2496556 | — |
| Reactant | (9-Hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde | HCID 86668369 | — |
| Product | HCID 67996053 | HCID 67996053 | 53% |
Reaction Steps
The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-(4-methoxy-phenyl)-propylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 53% of theory; LC (method 5): tR=1.02 min; Mass spectrum (ESI+): m/z=392 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765744B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-22a0121c75564533b401982799127ad9 |
| Source note | uspto-grants-2014_07 |