HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 7028357, compound → HCID 67996043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 7028357 | HCID 7028357 | — |
| Reactant | (9-Hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde | HCID 86668369 | — |
| Product | HCID 67996043 | HCID 67996043 | 55% |
Reaction Steps
The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-p-tolyl-propylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 55% of theory; LC (method 5): tR=1.10 min; Mass spectrum (ESI+): m/z=376 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765744B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-37eecf962bba497ea176b8835916a2b5 |
| Source note | uspto-grants-2014_07 |