HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Bromophenyl)cyclopropanamine → HCID 67996011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Bromophenyl)cyclopropanamine | HCID 18710195 | — |
| Reactant | (9-Hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde | HCID 86668369 | — |
| Product | HCID 67996011 | HCID 67996011 | 42% |
Reaction Steps
The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and 1-(4-bromo-phenyl)-cyclopropylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 42% of theory; LC (method 5): tR=1.12 min; Mass spectrum (ESI+): m/z=438/440 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765744B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-aeb97e45373d464db0628c7a2e963909 |
| Source note | uspto-grants-2014_07 |