(αS)-2-Chloro-α-methylbenzenemethanamine → HCID 70496706, compound

Participants

Reaction Steps

The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-(2-chloro-phenyl)-ethylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 89% of theory; LC (method 8): tR=1.18 min; Mass spectrum (ESI+): m/z=382/384 (Cl) [M+H]+.

Provenance & Evidence