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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1615155Generated: November 1, 2026

(1S)-1-phenylpropan-1-amine → HCID 70498234, compound

https://huagongshe.com/reaction/1615155

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(1S)-1-phenylpropan-1-amineHCID 6993773—
Reactant(9-Hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehydeHCID 86668369—
ProductHCID 70498234HCID 7049823450%

Reaction Steps

The title compound is prepared from (9-hydroxy-3,3-dimethyl-1,5-dioxa-spiro[5.5]undec-9-yl)-acetaldehyde and (S)-1-phenyl-propylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 50% of theory; LC (method 8): tR=1.16 min; Mass spectrum (ESI+): m/z=362 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765744B2
Source datasetuspto-grants-2014_07
ORD IDord-5969ccb1707f45ba95fc44edb647bb70
Source noteuspto-grants-2014_07