HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-(-)-1-(4-chlorophenyl)ethylamine → HCID 86668373, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-(-)-1-(4-chlorophenyl)ethylamine | HCID 1550852 | — |
| Reactant | HCID 86668374 | HCID 86668374 | — |
| Product | HCID 86668373 | HCID 86668373 | 75% |
Reaction Steps
The title compound is prepared from 2,2,2-trifluoro-N-[8-(2-oxo-ethyl)-1,4-dioxa-spiro[4.5]dec-8-yl]-acetamide and (S)-1-(4-chloro-phenyl)-ethylamine following a procedure analogous to that described in Step 3 of Intermediate 2. Yield: 75% of theory; LC (method 8): tR=1.10 min; Mass spectrum (ESI+): m/z=435/437 (Cl) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765744B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-ce9318f31f1e43fc9930c3c2d738103a |
| Source note | uspto-grants-2014_07 |