HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10214443, compound → HCID 178485261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10214443 | HCID 10214443 | — |
| Reactant | 1H-Indazole-6-carbaldehyde | HCID 18538368 | — |
| Product | HCID 178485261 | HCID 178485261 | — |
Reaction Steps
The title compound was synthesized from N-methyl-2-oxoindoline-5-carboxamide (11 mg, 0.0578 mmol) and 1H-indazole-6-carbaldehyde (10 mg, 0.0636 mmol) according to the method described for Example A1 to obtain 3.0 mg, 17%. 1H NMR (400 MHz, d6-DMSO) δ 13.33 (s, 1H), 10.88 (s, 1H), 8.24-8.22 (m, 1H), 8.18 (s, 2H), 7.93-7.88 (m, 2H), 7.84 (s, 1H), 7.72 (d, J=7.9 Hz, 1H), 7.46 (d, J=8.0 Hz, 1H), 6.91 (d, J=8.0 Hz, 1H), 2.68 (d, J=4.0 Hz, 3H); MS ESI 319.1 [M+H]+, calcd for [C18H14N4O2+H]+ 319.12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765748B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-8c2f1cd724a643ad972bbb2f3113e221 |
| Source note | uspto-grants-2014_07 |