6-Chloro-1,3-dihydroindol-2-one → HCID 178517231, compound

Participants

Reaction Steps

The title compound was synthesized according to the method described for Example A11B except substituting 6-chlorooxindole (30 mg, 0.179 mmol) and 1H-indazole-6-carbaldehyde (29 mg, 0.197 mmol) to obtain 22 mg (42%) of a yellow solid. 1H NMR (400 MHz, d6-DMSO) δ 13.30 (s, 1H), 10.79 (s, 1H), 8.16 (s, 1H), 7.90-7.87 (m, 2H), 7.83 (s, 1H), 7.56 (d, J=8.00 Hz, 1H), 7.41 (d, J=8.80 Hz, 1H), 6.93-6.88 (m, 2H); MS ESI 296.0 [M+H]+, calcd for [C16H10ClN3O+H]+ 296.06.

Provenance & Evidence