Divinyl sulfone → HCID 86691847, compound

Participants

Reaction Steps

To a solution of 38-4 (20 mg, 0.055 mmol) in ethanol (0.3 mL) at room temperature was added (ethenylsulfonyl)ethene (0.011 mL, 13 mg, 0.11 mmol). After 1 hour, the reaction was filtered and purified by reverse phase chromatography (1-100%, 0.1% TFA in H2O/Acetonitrile) to give desired product. MS (M+H)+: observed=482.2212, calculated=482.2220.

Provenance & Evidence