Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Hexachlorocyclotriphosphazene | HCID 220225 | — |
| Product | HCID 131731648 | HCID 131731648 | — |
Reaction Steps
Furthermore, into the 5-liter flask as described above is put a solution of hexachlorocyclotriphosphazene in toluene (700 g (6.0 unit mol) of hexachlorocyclotriphosphazene, 3,500 mL of toluene). The slurry solution of 2-methyl-2-proper-1-ol sodium salt is added dropwise thereto at 5° C. or lower over 6 hours, followed by warming to 25° C. and stirring for 4 hours, to obtain a solution of hexamethallylcyclotriphosphazene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08765878B2 |
|---|
| Source dataset | uspto-grants-2014_07 |
|---|
| ORD ID | ord-4ebaa8c3e1a84a47b8ae82294f37f2c9 |
|---|
| Source note | uspto-grants-2014_07 |
|---|
