反应详情

温度

60 °C

Into a 5-liter flask equipped with a reflux condenser, a thermometer, and a stirrer, 3,500 mL of toluene is weighed and put, and 707 g (6.2 mol) of 2-hepten-1-ol and 459 g (6.2 mol) of n-butyl alcohol are added thereto, followed by stirring until homogeneous. 74 g (3.2 gram atom) of metallic sodium is introduced thereto at 50° C. or lower, followed by warming to 60° C. over 1 hour after the completion of the introduction, and then stirring at from 60° C. to 68° C. for 4 hours to obtain a solution of 2-hepten-1-ol sodium salt and n-butyl alcohol sodium salt.

1. customInto a 5-liter flask equipped with a reflux condenser
2. customat 50° C.
3. stirringstirring at from 60° C. to 68° C. for 4 hours