HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dibromo-5,5-dimethylhydantoin → HCID 53307690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dibromo-5,5-dimethylhydantoin | HCID 6479 | — |
| Reactant | HCID 53307689 | HCID 53307689 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53307690 | HCID 53307690 | — |
Reaction Steps
To a solution of compound 13e (4.43 mg, 0.022 mmol) in CH3CN (44 μL) was added 1,3-dibromo-5,5-dimethylhydantoin (6.29 mg, 0.022 mmol) at room temperature. The resulting solution was stirred at room temperature for 10 minutes. The obtained material was easily degraded at temperature. Therefore, the 0.5 M CH3CN mixture reaction solution was used for next reaction without purification after confirmation of reaction color changing from clear to material specific deep red.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765920B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-c9d597c64f8f48049cb2f9e12c16dac9 |
| Source note | uspto-grants-2014_07 |