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HRID1616986

反应详情

EQUATION

反应方程式

HRID 1616986 的结构方程式

REACTANTS

反应物

2
结构：Cc1cccc(C)c1O
HCID11335

2,6-Dimethylphenol

C8H10O

结构：O=c1[nH]n(-c2ccc(O)cc2)c(=O)n1-c1ccccc1
HCID67258169

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(-n2[nH]c(=O)n(-c3ccccc3)c2=O)cc(C)c1O
HCID67258590

未命名化合物

PROCEDURE

实验过程

Compound 30 was prepared from 2,6-dimethylphenol in the same manner of compound 27, and was obtained as white solids (61%). 1H NMR (300 MHz, DMSO-d6): δ 11.32 (br s, 1H), 8.42 (s, 1H), 7.53-7.39 (m, 5H), 7.14 (d, J=1.8 Hz, 1H). 13C NMR (75 MHz, DMSO-d6): δ 152.07, 151.38, 129.58, 127.13, 125.61, 121.94, 121.48, 17.43. HRMS: calcd for C16H15N3O3 (MH+) 298.1186. found 298.1184.