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HRID1617169

反应详情

EQUATION

反应方程式

HRID 1617169 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CO
HCID887

Methanol

CH4O

结构：CCCCCNc1nc(N)nc(C)c1CCCNC(=O)Cc1ccc(CC(=O)O)cc1
HCID68415389

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCNc1nc(N)nc(C)c1CCCNC(=O)Cc1ccc(CC(=O)OC)cc1
HCID42613075

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

The product from step (i) was dissolved in MeOH (20 mL) then a solution of HCl in dioxane (4M, 0.3 ml) was added and stirred overnight. Solvent was removed and the residue purified by RPHPLC to afford the title compound, 0.032 g.

WORKUP

后处理

  1. customSolvent was removed
  2. customthe residue purified by RPHPLC