反应详情

A mixture of the product from step (iv) (0.3 g) and butylamine (1 ml) in 1,4-dioxane (6 ml) was sealed into a microwave tube and the reaction was performed in the CEM Microwave, at 160° C. and 100 W for 1 h. The solvent was evaporated under reduced pressure and the residue used crude in the next step.

1. customwas sealed into a microwave tube
2. customwas performed in the CEM Microwave, at 160° C.
3. customThe solvent was evaporated under reduced pressure