HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86688554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86688555 | HCID 86688555 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86688554 | HCID 86688554 | — |
Reaction Steps
To 4.30 g (13.9 mmol) 6-Ethoxy-3′,4′,5′,6′-tetrahydro-2′H-[3,4]bipyridinyl-1′-carboxylic acid tert-butyl ester (VII.1) in 10 mL EtOAc are added 120 mL 4N HCl in EtOAc. The mixture is stirred for 12 h at rt. After that time, the solvent is evaporated to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765959B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-80063d9005364dac9583896e9df615b0 |
| Source note | uspto-grants-2014_07 |