Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617444Generated: November 3, 2026

Hydroxyamine hydrochloride → HCID 136359962, compound

https://huagongshe.com/reaction/1617444

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 66667109HCID 66667109—
ProductHCID 136359962HCID 136359962—

Reaction Steps

In analogy to example 1, step 2, from 3-(3-bromo-phenyl)-3-o-tolyl-1-pyridin-4-yl-propan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (3:1) as a white foam, MS (ESI+): m/z=395.0 ([M+H]+, 1Br).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-4912369654db43a8abc5e440c90e1256
Source noteuspto-grants-2014_07