Phenylboronic Acid → HCID 66666709, compound

HRID 1617445Notes

Reaction equation

HRID 1617445 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([CH:8]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=2C)[CH2:9][C:10]([C:13]2[CH:18]=[CH:17][N:16]=[CH:15][CH:14]=2)=NO)[CH:5]=[CH:6][CH:7]=1.C1(B(O)[OH:33])C=CC=CC=1>>[Br:1][C:2]1[CH:3]=[C:4]([CH:8]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH2:9][C:10]([C:13]2[CH:18]=[CH:17][N:16]=[CH:15][CH:14]=2)=[O:33])[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 66827Phenylboronic AcidHCID 136359962HCID 136359962, compound

Product 1

HCID 66666709HCID 66666709, compound

Procedure

In analogy to example 1, step 1, from (E)-3-(3-bromo-phenyl)-1-pyridin-4-yl-propenone (example 11) and phenylboronic acid was prepared the title compound as a colorless oil, MS (ESI+): m/z=380.1 ([M+H]+, 1Br).

Sources & evidence

ORD record
ord-1520f5ace059411bb149aa1088a2e646
Source dataset
uspto-grants-2014_07
Patent number
US08765730B2

Reaction notes

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