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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617463Generated: October 31, 2026

Hydroxyamine hydrochloride → HCID 136359968, compound

https://huagongshe.com/reaction/1617463

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 66666379HCID 66666379—
ProductHCID 136359968HCID 136359968—

Reaction Steps

In analogy to example 1, step 2, from 3-(4-bromo-phenyl)-1-pyridin-4-yl-3-o-tolyl-propan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (2.5:1) as a white foam, MS (ESI+): m/z=395.1 ([M+H]+, 1Br).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-b49f9122a6d04a6996fdd65295177f57
Source noteuspto-grants-2014_07