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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617472Generated: November 1, 2026

Hydroxyamine hydrochloride → HCID 136359973, compound

https://huagongshe.com/reaction/1617472

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 86660936HCID 86660936—
ProductHCID 136359973HCID 136359973—

Reaction Steps

In analogy to example 1, step 2, from 3-(4-bromo-phenyl)-1-(2-chloro-pyridin-4-yl)-3-phenyl-propan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (2.6:1) as a colorless oil, MS (ESI−): m/z=413.0 ([M−H]−, 1Br,1Cl).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-2abf58cce9724dcea7b4c5965717b647
Source noteuspto-grants-2014_07