HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 136359973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 86660936 | HCID 86660936 | — |
| Product | HCID 136359973 | HCID 136359973 | — |
Reaction Steps
In analogy to example 1, step 2, from 3-(4-bromo-phenyl)-1-(2-chloro-pyridin-4-yl)-3-phenyl-propan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (2.6:1) as a colorless oil, MS (ESI−): m/z=413.0 ([M−H]−, 1Br,1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-2abf58cce9724dcea7b4c5965717b647 |
| Source note | uspto-grants-2014_07 |