HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 87237114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Reactant | 1-(2,6-Dichloropyridin-4-YL)ethanone | HCID 22119446 | — |
| Product | HCID 87237114 | HCID 87237114 | — |
Reaction Steps
In analogy to example 11, step 1, from 4-bromobenzaldehyde and 1-[2,6-dichloropyridin-4-yl]ethanone (CAS RN: [185319-20-4]) was prepared 3-(4-bromo-phenyl)-1-(2,6-dichloro-pyridin-4-yl)-propenone as a yellow solid, which was directly subjected to the next step. In analogy to example 1, step 1, from 3-(4-bromo-phenyl)-1-(2,6-dichloro-pyridin-4-yl)-propenone and phenylboronic acid was prepared the title compound as a colorless oil, MS (EI+): m/z=433 ([M]+, 1Br, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-bd8d375d5c224950a8d470938ddf92e3 |
| Source note | uspto-grants-2014_07 |