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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617475Generated: October 31, 2026

Hydroxyamine hydrochloride → HCID 76671396, compound

https://huagongshe.com/reaction/1617475

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 66668679HCID 66668679—
ProductHCID 76671396HCID 76671396—

Reaction Steps

In analogy to example 1, step 2, from 3-(4-bromo-phenyl)-1-(2,5-dichloro-phenyl)-3-o-tolyl-propan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (2.4:1) as a white foam, MS (EI): m/z=463 ([M]+, 1Br).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-3107b2d16ab44d5291e4dd86c3a66fc9
Source noteuspto-grants-2014_07