HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanamine, N-methoxy-, hydrochloride (1:1) → 2-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-N-methoxy-N-methyl-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanamine, N-methoxy-, hydrochloride (1:1) | HCID 81138 | — |
| Reactant | 10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-ylacetic acid | HCID 12669091 | — |
| Product | 2-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-N-methoxy-N-methyl-acetamide | HCID 86660944 | — |
Reaction Steps
In analogy to example 55, step 1, from 10,11-dihydro-5H-dibenzo[a,d]cycloheptene-5-acetic acid (CAS RN: [4037-50-7]) and N,O-dimethylhydroxylamine hydrochloride was prepared the title compound as a colorless oil, MS (ESI+): m/z=296.3 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-9d8e9ec99b25469bac4e892c7bb2cd73 |
| Source note | uspto-grants-2014_07 |