HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodopyridine → 2-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-1-pyridin-4-yl-ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodopyridine | HCID 609492 | — |
| Reactant | 2-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-N-methoxy-N-methyl-acetamide | HCID 86660944 | — |
| Product | 2-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-1-pyridin-4-yl-ethanone | HCID 67015505 | — |
Reaction Steps
In analogy to example 55, step 2, from 2-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-N-methoxy-N-methyl-acetamide and 4-iodopyridine was prepared the title compound as a white solid, MS (ESI+): m/z=314.1 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-8176f2e3176b48049ed15ad8b33a783a |
| Source note | uspto-grants-2014_07 |