HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanamine, N-methoxy-, hydrochloride (1:1) → 2-(9H-Fluoren-9-yl)-N-methoxy-N-methyl-acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanamine, N-methoxy-, hydrochloride (1:1) | HCID 81138 | — |
| Edukt | Fluorene-9-acetic acid | HCID 94852 | — |
| Produkt | 2-(9H-Fluoren-9-yl)-N-methoxy-N-methyl-acetamide | HCID 86660945 | — |
Reaktionsschritte
In analogy to example 55, step 1, from fluorene-9-acetic acid (CAS RN: [6284-80-6]) and N,O-dimethylhydroxylamine hydrochloride was prepared the title compound as an off-white oil, MS (ESI+): m/z=268.1 ([M+H]+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08765730B2 |
| Quelldatensatz | uspto-grants-2014_07 |
| ORD ID | ord-a7deb74daa8446ff849481a1cf55acff |
| Quellennotiz | uspto-grants-2014_07 |