HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → 2-(9H-Fluoren-9-yl)-1-pyridin-4-yl-ethanone oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-(9H-Fluoren-9-yl)-1-pyridin-4-yl-ethanone | HCID 66666573 | — |
| Product | 2-(9H-Fluoren-9-yl)-1-pyridin-4-yl-ethanone oxime | HCID 136359977 | — |
Reaction Steps
In analogy to example 1, step 2, from 2-(9H-fluoren-9-yl)-1-pyridin-4-yl-ethanone and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (1:1) as a white foam, MS (ESI+): m/z=301.3 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-829cea064f5447e689c3476502a9b03c |
| Source note | uspto-grants-2014_07 |