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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617521Generated: October 29, 2026

Hydroxyamine hydrochloride → HCID 136359992, compound

https://huagongshe.com/reaction/1617521

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 67015515HCID 67015515—
ProductHCID 136359992HCID 136359992—

Reaction Steps

In analogy to example 74, step 7, from 3-{4-[3-(2-methyl-pyridin-4-yl)-3-oxo-1-o-tolyl-propyl]-phenyl}-acrylic acid and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of Z to E isomers (1.7:1) as a colorless oil, MS (ESI+): m/z=401.1859 ([M+H]+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-8b52525f83454d09a8f050e872242684
Source noteuspto-grants-2014_07