HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanamine, N-methoxy-, hydrochloride (1:1) → 3-(3-Bromo-phenyl)-N-methoxy-N-methyl-3-o-tolyl-propionamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanamine, N-methoxy-, hydrochloride (1:1) | HCID 81138 | — |
| Reactant | 3-(3-Bromo-phenyl)-3-o-tolyl-propionic acid | HCID 66666809 | — |
| Product | 3-(3-Bromo-phenyl)-N-methoxy-N-methyl-3-o-tolyl-propionamide | HCID 86660965 | — |
Reaction Steps
In analogy to example 74, step 4, from 3-(3-bromo-phenyl)-3-o-tolyl-propionic acid and N,O-dimethylhydroxylamine hydrochloride was prepared the title compound as a white solid, mp 89° C., MS (ESI+): m/z=362.07 ([M+H]+, 1 Br).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-4bc9220772a24534bf78a8a2a46d4144 |
| Source note | uspto-grants-2014_07 |