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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617548Generated: October 31, 2026

Hydroxyamine hydrochloride → HCID 136360003, compound

https://huagongshe.com/reaction/1617548

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 66665958HCID 66665958—
ProductHCID 136360003HCID 136360003—

Reaction Steps

In analogy to example 74, step 7, from 3-[3-(3-hydroxy-propyl)-phenyl]-1-(2-methyl-pyridin-4-yl)-3-o-tolyl-propan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (3:1) as a colorless oil, MS (ESI+): m/z=389.2 ([M+H]+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-daf6516a96124f0180baa922b45000bf
Source noteuspto-grants-2014_07