Hydroxyamine hydrochloride → HCID 136360008, compound

Participants

Reaction Steps

In analogy to example 74, step 7, from 3-(4-bromo-phenyl)-5-methyl-1-pyridin-4-yl-hexan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (2.7:1) as a colorless oil, MS (ESI+): m/z=361.2 ([M+H]+, 1Br).

Provenance & Evidence