Hydroxyamine hydrochloride → HCID 136360015, compound

Participants

Reaction Steps

In analogy to example 74, step 7, from 3-(4-bromo-phenyl)-1-(2-fluoro-5-methyl-pyridin-4-yl)-4,4-dimethyl-pentan-1-one and hydroxylamine hydrochloride in the presence of NaHCO3 was prepared the title compound as a mixture of E and Z isomers (3.7:1) as a white foam, MS (ESI+): m/z=375.1062 ([M+H]+, 1Br).

Provenance & Evidence