HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 136166981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 66669058 | HCID 66669058 | — |
| Product | HCID 136166981 | HCID 136166981 | — |
Reaction Steps
In analogy to example 151, step 3, 2-methyl-3,3-diphenyl-1-pyridin-4-yl-propan-1-one was reacted with hydroxylamine hydrochloride in the presence of NaHCO3 to give the title compound as an off-white solid, MS (ESI+): m/z=317.16 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-6444f2fdf4294ee496a049b98781fce9 |
| Source note | uspto-grants-2014_07 |