HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 87237018, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 67015650 | HCID 67015650 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 87237018 | HCID 87237018 | — |
Reaction Steps
In analogy to example 151, step 3, 4-{4-[3-(1-methyl-6-oxo-1,6-dihydro-pyridin-3-yl)-3-oxo-1-o-tolyl-propyl]-benzoylamino}-butyric acid was reacted with hydroxylamine hydrochloride in ethanol and water in the presence of NaHCO3 to give the title compound as a colorless solid, MS (ESI+): m/z=504.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-986c559f337f4c0c9b55bdaca5fd9f2c |
| Source note | uspto-grants-2014_07 |