Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylpyridine → (R)-4-(4-Bromophenyl)-1-(pyridin-2-yl)-4-o-tolylbutan-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylpyridine | HCID 7975 | — |
| 반응물 | (R)-3-(4-Bromophenyl)-N-methoxy-N-methyl-3-o-tolylpropanamide | HCID 71813344 | — |
| 생성물 | (R)-4-(4-Bromophenyl)-1-(pyridin-2-yl)-4-o-tolylbutan-2-one | HCID 67015648 | — |
반응 단계
In analogy to example 261, step 1, from (R)-3-(4-bromophenyl)-N-methoxy-N-methyl-3-o-tolylpropanamide (example 142, step 1) and 2-methyl-pyridine was prepared the title compound as a yellow oil, MS (ESI+): m/z=394.0 ([M+H]+, 1Br).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08765730B2 |
| 출처 데이터셋 | uspto-grants-2014_07 |
| ORD ID | ord-2f3f698a867c41e8b2d82dce77d97d9a |
| 출처 메모 | uspto-grants-2014_07 |