HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66668328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67015779 | HCID 67015779 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66668328 | HCID 66668328 | — |
Reaction Steps
In analogy to example 162, step 2, (E)-3-(4-chloro-2-fluorophenyl)-1-(6-methoxypyridin-3-yl)prop-2-en-1-one (example 237, step 1) was reacted with concentrated aqueous HCl in 1,4-dioxane to give the title compound as an colourless solid, MS (ESI+): m/z=278.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-e0af8e3cb0134a1396ebedc37a565202 |
| Source note | uspto-grants-2014_07 |