HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66666764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66666270 | HCID 66666270 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66666764 | HCID 66666764 | — |
Reaction Steps
In analogy to example 162, step 2, ethyl 3-(1-(4-chloro-2-fluorophenyl)-3-(6-methoxy-pyridin-3-yl)-3-oxopropyl)benzoate was reacted with concentrated aqueous HCl in 1,4-dioxane to give the title compound as an colourless solid, MS (ESI+): m/z=426.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-003b46cb35e04f9e88c729ae6f4afd46 |
| Source note | uspto-grants-2014_07 |