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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1617937Generated: November 3, 2026

Hydroxyamine hydrochloride → HCID 58043620, compound

https://huagongshe.com/reaction/1617937

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 66668714HCID 66668714—
ProductHCID 58043620HCID 58043620—

Reaction Steps

In analogy to example 151, step 3, 5-{4-[1-(4-chloro-2-methyl-phenyl)-3-(1-methyl-6-oxo-1,6-dihydro-pyridin-3-yl)-3-oxo-propyl]-phenoxy}-2-fluoro-benzoic acid was reacted with hydroxylamine hydrochloride in the presence of sodium hydrogencarbonate to give the title compound as a colourless solid, MS (ESI−): m/z=533.1 [M−H]−.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765730B2
Source datasetuspto-grants-2014_07
ORD IDord-106845b22c514d159154a8baee240187
Source noteuspto-grants-2014_07