HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → (E)-5-(3-(2,5-Dichlorophenyl)acryloyl)-1-methylpyridin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (E)-5-(3-(2,5-dichlorophenyl)acryloyl)pyridin-2(1H)-one | HCID 66668831 | — |
| Product | (E)-5-(3-(2,5-Dichlorophenyl)acryloyl)-1-methylpyridin-2(1H)-one | HCID 66668982 | — |
Reaction Steps
In analogy to example 161, step 1, (E)-5-(3-(2,5-dichlorophenyl)acryloyl)pyridin-2(1H)-one was reacted with iodomethane in the presence of potassium carbonate to give the title compound as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-cdf6892a685a4cc69e8377eb7e2d5b9a |
| Source note | uspto-grants-2014_07 |