HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 66668223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 66668187 | HCID 66668187 | — |
| Product | HCID 66668223 | HCID 66668223 | — |
Reaction Steps
In analogy to example 161, step 1, (E)-5-(3-(3,5-difluorophenyl)acryloyl)pyridin-2(1H)-one was reacted with iodomethane in the presence of potassium carbonate to give the title compound as a light yellow solid. MS (ESI+): m/z=276.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765730B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-2ce3829055a845fba239d2183d06566b |
| Source note | uspto-grants-2014_07 |