HCID 59631403, compound → HCID 59631071, compound

HRID 1618517Notes

Reaction equation

HRID 1618517 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([NH:8][C:9]([CH:11]([CH:17]([CH3:19])[CH3:18])[C:12]([O:14]CC)=[O:13])=[O:10])[CH:5]=[CH:6][CH:7]=1>C1COCC1>[F:1][C:2]1[CH:3]=[C:4]([NH:8][C:9]([CH:11]([CH:17]([CH3:19])[CH3:18])[C:12]([OH:14])=[O:13])=[O:10])[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 59631403HCID 59631403, compound

Product 1

HCID 59631071HCID 59631071, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Prepared according to procedure B using ethyl 2-(3-fluorophenylcarbamoyl)-3-methylbutanoate (5.2 g, 19.45 mmol) in THF (20 mL) to give 2-(3-fluorophenylcarbamoyl)-3-methylbutanoic acid as a white solid.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-c180cd8cc9ca4818bb8849af9696cd4e
Source dataset
uspto-grants-2014_07
Patent number
US08765940B2

Reaction notes

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