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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1618579Generated: November 1, 2026

Phosphorus oxychloride → HCID 67285129, compound

https://huagongshe.com/reaction/1618579

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphorus oxychlorideHCID 24813—
ReactantHCID 178486796HCID 178486796—
ProductHCID 67285129HCID 67285129—

Reaction Steps

Prepared according to procedure S using 7-methoxy-2,3,6-trimethylquinolin-4-ol (444.7 mg, 2.0 mmol) and POCl3 (2.0 mL, 21.5 mmol) to give 4-chloro-7-methoxy-2,3,6-trimethylquinoline. Mass Spectrum (ESI), m/e=236.1 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765940B2
Source datasetuspto-grants-2014_07
ORD IDord-3a8b4117e1084932b6df132bfd046879
Source noteuspto-grants-2014_07