HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-methylacetoacetate → HCID 178426077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-methylacetoacetate | HCID 701 | — |
| Reactant | 2-Chloro-p-toluidine | HCID 12007 | — |
| Product | HCID 178426077 | HCID 178426077 | — |
Reaction Steps
Prepared according to procedure R using 2-chloro-4-methyl-aniline (2.0 mL, 16.3 mmol), ethyl-2-methyl-acetoacetate (4.6 mL, 32.5 mmol), and PPA (8.12 g, 81.2 mmol) to afford 8-chloro-2,3,6-trimethylquinolin-4-ol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-7239a892cfd243dbaeba184879f9810f |
| Source note | uspto-grants-2014_07 |