HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-methylacetoacetate → HCID 178493406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-methylacetoacetate | HCID 701 | — |
| Reactant | 2,4-Dimethoxyaniline | HCID 17652 | — |
| Product | HCID 178493406 | HCID 178493406 | — |
Reaction Steps
Prepared according to procedure R using 2,4-dimethoxy aniline (1.99 g, 13.0 mmol), ethyl-2-methyl-acetoacetate (3.7 mL, 26.2 mmol), and PPA (6.78 g, 67.8 mmol) to afford 6,8-dimethoxy-2,3-dimethylquinolin-4-ol. Mass Spectrum (ESI) m/e=234.1 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-174fddb71dfa4e1a94464fc6ddea61fc |
| Source note | uspto-grants-2014_07 |