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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1618584Generated: November 3, 2026

Phosphorus oxychloride → HCID 54891680, compound

https://huagongshe.com/reaction/1618584

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphorus oxychlorideHCID 24813—
ReactantHCID 178493406HCID 178493406—
ProductHCID 54891680HCID 54891680—

Reaction Steps

Prepared according to procedure S using 6,8-dimethoxy-2,3-dimethylquinolin-4-ol (1.0 g, 7.0 mmol) and POCl3 (5.0 mL, 53.6 mmol) to afford 4-chloro-6,8-dimethoxy-2,3-dimethylquinoline. Mass Spectrum (ESI) m/e=252.1 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08765940B2
Source datasetuspto-grants-2014_07
ORD IDord-9b3382da02ee467a9dee27d4713d2764
Source noteuspto-grants-2014_07