HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → HCID 178489314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | Ethyl (2-methoxybenzoyl)acetate | HCID 2759695 | — |
| Product | HCID 178489314 | HCID 178489314 | — |
Reaction Steps
Prepared according to procedure R using 4-chloroaniline (774.0 mg, 6.1 mmol), ethyl (2-methoxybenzoyl)acetate (2.0 mL, 10.3 mmol), and PPA (4.70 g, 47.0 mmol) to afford 6-chloro-2-(2-methoxyphenyl)quinolin-4-ol. Mass Spectrum (ESI) m/e=286.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-7c3f9b59b30741ee9eb6034fc9151dbb |
| Source note | uspto-grants-2014_07 |