HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-methylacetoacetate → HCID 178432160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-methylacetoacetate | HCID 701 | — |
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Product | HCID 178432160 | HCID 178432160 | — |
Reaction Steps
Prepared according to procedure R using 4-chloroaniline (2 g, 15.68 mmol) and ethyl 2-methyl-3-oxobutanoate (4.53 mL, 31.36 mol) to give 6-chloro-2,3-dimethylquinolin-4-ol as a white solid: Mass Spectrum (ESI) m/e=208.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-948468e31673465089063ec5f388154a |
| Source note | uspto-grants-2014_07 |