HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → HCID 178427869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | Ethyl 2-methyl-4,4,4-trifluoroacetoacetate | HCID 2737204 | — |
| Product | HCID 178427869 | HCID 178427869 | — |
Reaction Steps
Prepared according to procedure R using 4-chloroaniline (6.44 g, 50.47 mmol) and ethyl 4,4,4-trifluoro-2-methyl-3-oxobutanoate (10 g, 50.47 mmol) to give 6-chloro-3-methyl-2-(trifluoromethyl)quinolin-4-ol as an off-white solid: Mass Spectrum (ESI) m/e=262.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-d444e1bd62e1464193fd19873f4905c7 |
| Source note | uspto-grants-2014_07 |